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Table 1 Flexlab set up for radiolabelling reactions

From: Automated synthesis of 18F radiolabelled indole containing Oncrasin-like molecules; a comparison of iodonium salts and boronic ester chemistry

Container Reagents
Vial 1 Eluent
Vial 2 4 mg of precursor in 500 μl of DMF
Vial 3 1 ml anhydrous acetonitrile
Vial 4 450 μl of DMF. 50 μl of Pyridine, 15 mg of Cu(OTf)2
Vial 5 1 ml of Acetonitrile and 1 ml of distilled water
Vial 6  
Vial 7  
Vial 8  
Vial 9  
Vial 10  
Vial 11 10 ml of distilled water
Vial 12 1 ml of ethanol
Vial 13 1 ml of saline
Vial 14  
Vial 15  
Vial 16  
Vial 17  
Vial 18  
Vial 19  
QMA seppak Quaternary Methyl Ammonium Cartridge
Seppak A  
Seppak B  
Seppak C  
Seppak D C18 seppak
HPLC Vial 1  
HPLC Vial 2 40 ml of distilled water
Reactor 1 1 ml anhydrous acetonitrile
Reactor 2  
Loop Vial 1  
Loop Vial 2 1 ml distilled water
HPLC eluent A 0.1% Ammonium formate
HPLC eluent B Acetonitrile
HPLC eluent C Water
HPLC eluent D Ethanol