Table 7 RCY and RCP Production of clinical batches (after t = 0, 4, 24 and 48 h)
RCY (%), Radio-TLC-scanner | RCY (%), Gamma counter | RCP (%), HPLC | |||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|
t0 | t4 | t24 | t48 | t0 | t4 | t24 | t48 | t0 | t4 | t24 | t48 |
Syringe | |||||||||||
> 99.9 | > 99.9 | > 99.9 | > 99.9 | > 99.9 | > 99.9 | 99.8 ± 0.1 | 99.5 | 97.9 ± 0.1 | 97.5 ± 0.1 | 94.4 ± 0.1 | 90.8 ± 0.4 |
Flask | |||||||||||
99.5 ± 0.5 | 99.3 ± 0.5 | 99.7 ± 0.3 | 99.4 ± 0.6 | 98.6 ± 1.6 | > 99.9 | 98.7 ± 1.3 | 99.3 ± 0.9 | 97.3 ± 0.7 | 96.5 ± 0.5* | 92.8 ± 0.7 | 88.0 ± 2.7 |