Solvent 0.5 mL |
Precursor (μmol) |
Temperature (°C) |
Kryptofix (μmol) |
K2CO3 (μmol) |
Yield (%) |
---|---|---|---|---|---|
DMSO | 26 | 120 | 6 | 3 | 6% |
DMSO | 24 | 140 | 6 | 3 | 7% |
DMSO | 54 | 140 | 6 | 3 | 5% |
DMSO | 26 | 160 | 6 | 3 | 4% |
MeCN | 26 | 140 | 6 | 3 | 1% |
MeCN | 24 | 140 | 18 | 9 | 2% |
DMSO | 16 | 140 | 6 | 3 | 3% |